Presentation and Photolytic synthesis

28 Setembro 2016, 16:00 • Christopher David Maycock

Presentation of rules for the lab course. Use of lab-coat, Eye protection and general attention to safety in the laboratory. Formation of groups and start of the photolytic synthesis of benzopinacol using sunlight. Each student has a lab book. Experiment list:

Bloco 1

 

1. Sintese de Benzopinacol                                          Vogel P. 528 (method A) (1 aula)

 

2. Sintese de 7,7-Diclorobiciclo[4.1.0]heptano            Vogel P. 1110 (1 aula)

 

3. Sintese de 1,1’-Bi-2-naftol                                      Vogel P. 838 (1 aula)

 

4. Sintese de Ciclohexeno                                           Vogel P.491 (1 aula)

 

Bloco 2

 

5. ver folha      Sintese de 2-Amino-5-iodopiridina

 

6.ver folha       Sintese de 2-Cloro-5-iodopiridina

After experiment 1 the experiments will be rotated such that in the second lab, group 1 will do expt. 2, group 3 expt. 3, group 4 and 5 expt. 4. 

After finishing Block 1 all groups will do the block 2 experiments simultaneously.